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Research on nitrogen and sulfur heterocyclic compounds: Synthesis of 10H‐pyrrolo[1,2‐a]thieno[3,4‐e][1,4]‐diazepin‐5(4H)‐one and some derivatives

Identifieur interne : 001459 ( France/Analysis ); précédent : 001458; suivant : 001460

Research on nitrogen and sulfur heterocyclic compounds: Synthesis of 10H‐pyrrolo[1,2‐a]thieno[3,4‐e][1,4]‐diazepin‐5(4H)‐one and some derivatives

Auteurs : Abdelali Daich [France] ; Jean Morel [France] ; Bernard Decroix [France]

Source :

RBID : ISTEX:4A2BA0EDC5F6EFFB50D8D69A8C50092DD9E9A77E

Abstract

The synthesis of 10H‐pyrrolo[1,2‐a]thieno[3,4‐e][1,4]diazepin‐5(4H)‐one (16) and some derivatives are described from methyl 3‐bromomethylthiophene‐4‐carboxylate (5). The key step of these sequences is the intramolecular cyclization of the carbonylazides 12 and 13.

Url:
DOI: 10.1002/jhet.5570310214


Affiliations:


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ISTEX:4A2BA0EDC5F6EFFB50D8D69A8C50092DD9E9A77E

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